4-(4-bromophenyl)-4-hydroxycyclohexanone synthesis
- Product Name:4-(4-bromophenyl)-4-hydroxycyclohexanone
- CAS Number:1477524-71-2
- Molecular formula:C12H13BrO2
- Molecular Weight:269.13
Yield:1477524-71-2 92%
Reaction Conditions:
Stage #1: 1.4-dibromobenzenewith n-butyllithium in tetrahydrofuran;hexane at 0;Flow reactor;
Stage #2: 1,4-Cyclohexanedione in tetrahydrofuran;hexane at 0;Flow reactor;
References:
Kim, Heejin;Lee, Hyune-Jea;Kim, Dong-Pyo [Angewandte Chemie - International Edition,2016,vol. 55,# 4,p. 1422 - 1426][Angew. Chem.,2016,vol. 128,# 4,p. 1444 - 1448,5] Location in patent:supporting information
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125962-59-6
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106-37-6
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1477524-71-2
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![1,4-Dioxaspiro[4.5]decan-8-one](/CAS/GIF/4746-97-8.gif)
4746-97-8
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1477524-71-2
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