2,2'-Dipicolylamine

2,2'-Dipicolylamine Suppliers list

Company Name:	Shanghai Wishpharma Co.,Ltd. Gold
Tel:	021-56789108 18550363168
Email:	95413064@qq.com

Company Name:	Guangdong RUNXING Biotechnology Company Limited Gold
Tel:	18516234359
Email:	1398175781@qq.com

Company Name:	Z IntellecChem & Tech. Co., Ltd Gold
Tel:	13179383568; 15050866711
Email:	contact@zintellec.com

Company Name:	Changzhou Jianuokang Pharmaceutical Co., Ltd. Gold
Tel:	0519-85202684; 13775120798
Email:	jnkpharmtech@163.com

2,2'-Dipicolylamine manufacturers

2,2'-Dipicolylamine Basic information

Product Name:	2,2'-Dipicolylamine
Synonyms:	Bis-pyridin-2-ylmethyl-amine;2,2''-(IMINODIMETHYLENE)DI- PYRIDINE;2,2''-DIPICOLYLAMINE 95+%;Bis((pyridin-2-yl)methyl)amine ,95%;2,2'-Iminobismethylenebispyridine;Bis(pyridine-2-ylmethyl)amine;N-(2-Pyridinylmethyl)-2-pyridinemethanamine;2-PyridineMethanaMine, N-(2-pyridinylMethyl)-
CAS:	1539-42-0
MF:	C12H13N3
MW:	199.25
EINECS:	216-266-8
Product Categories:	C9 to C46;Heterocyclic Building Blocks;Pyridines;Heterocyclic Compounds;Building Blocks;C12;Chemical Synthesis;Heterocyclic Building Blocks;1
Mol File:	1539-42-0.mol

2,2'-Dipicolylamine Chemical Properties

Boiling point	139-141 °C/1 mmHg (lit.)
density	1.107 g/mL at 25 °C (lit.)
refractive index	n20/D 1.578(lit.)
Fp	>230 °F
storage temp.	under inert gas (nitrogen or Argon) at 2–8 °C
solubility	water: soluble (partially miscible)(lit.)
form	clear liquid
pka	5.89±0.20(Predicted)
color	White to Yellow to Green
Water Solubility	water: soluble (partially miscible)(lit.)
InChI	InChI=1S/C12H13N3/c1-3-7-14-11(5-1)9-13-10-12-6-2-4-8-15-12/h1-8,13H,9-10H2
InChIKey	KXZQYLBVMZGIKC-UHFFFAOYSA-N
SMILES	C1(CNCC2=NC=CC=C2)=NC=CC=C1
EPA Substance Registry System	2,2'-Dipicolylamine (1539-42-0)

Safety Information

MSDS Information

Provider	Language
SigmaAldrich	English

2,2'-Dipicolylamine Usage And Synthesis

Chemical Properties	Yellow liquid
Uses	2,2'-Dipicolylamine is a metal chelators and a potential MBL inhibitors.
Synthesis	In a 100mL three-necked flask, 2-formylpyridine (10mmol) was added, and under stirring conditions, 20mL of methanol solution of 2-aminomethylpyridine (10mmol) was added dropwise to 2-formylpyridine, and stirred at room temperature for 10h after the dropwise addition was completed. NaBH4 (20mmol) was added to the reaction system in several portions and slowly, and the reaction solution turned from brown to light yellow, and stirred at room temperature overnight. Light yellow, stirring at room temperature overnight, evaporate the solvent under reduced pressure, then add 20mL distilled water, under stirring with 32% dilute hydrochloric acid to pH neutral, extracted with dichloromethane (3 30mL), collect the lower layer of the yellow solution with anhydrous MgSO4 drying, distillation under reduced pressure to obtain a yellow liquid, the yield of 95%.

2,2'-Dipicolylamine Preparation Products And Raw materials

Raw materials	Ethanol-->Ethyl acetate-->Potassium carbonate-->Sodium sulfate-->Triethylamine-->Palladium-->Methylamine-->2-Cyanopyridine-->2-(Chloromethyl)pyridine hydrochloride-->2-(Hydroxymethyl)pyridine-->2-(Bromomethyl)pyridine hydrobromide-->2-Pyridinemethanamine, N-(2-pyridinylmethylene)--->2-Picolylamine
Preparation Products	1,2-Ethanediamine, N,N-bis(2-pyridinylmethyl)-

Tag:2,2'-Dipicolylamine(1539-42-0) Related Product Information

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